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학술논문펄프종이기술2013.10 발행

속실렛 추출법에 의한 밀랍지의 탈랍처리 효과분석

Effect of Soxhlet Extraction Condition on Dewaxing Efficiency of the Beeswax-Treated Paper

최경화(강원대학교); 장혜미(한듬문화재)

45권 5호, 64~70쪽

초록

In this study, the effect of soxhlet extraction on dewaxing of the aged beeswax-treated paper was examined. To do this, soxhlet extraction of the aged beeswax-treated paper performed with different reflux conditions and then measured the dewaxing efficiency and change in the various properties such as tensile strength, folding endurance, color and brightness. Also, an artificial aging test was executed in order to investigate the effect of soxhlet extraction on the preservability of the dewaxed paper. As the result of FT-IR analysis, a peak area of CH and COOH group, which are main band of beeswax, was decreased or removed after soxhlet extraction. The decreasing rate of each peaks were increased depending on reflux time. After dewaxing, the physical property such as MIT type folding endurance and tensile strength was decreased. And L* value and brightness were increased while a* and b* value were decreased due to the remove of color compounds in beeswax. The more color deviation (ΔE) is expected with higher reflux times. As the result of artificial aging, preservability of two dewaxed papers except of DP_SE(C) sample was higher than that of untreated paper i.e. beeswax-treated paper.

Abstract

In this study, the effect of soxhlet extraction on dewaxing of the aged beeswax-treated paper was examined. To do this, soxhlet extraction of the aged beeswax-treated paper performed with different reflux conditions and then measured the dewaxing efficiency and change in the various properties such as tensile strength, folding endurance, color and brightness. Also, an artificial aging test was executed in order to investigate the effect of soxhlet extraction on the preservability of the dewaxed paper. As the result of FT-IR analysis, a peak area of CH and COOH group, which are main band of beeswax, was decreased or removed after soxhlet extraction. The decreasing rate of each peaks were increased depending on reflux time. After dewaxing, the physical property such as MIT type folding endurance and tensile strength was decreased. And L* value and brightness were increased while a* and b* value were decreased due to the remove of color compounds in beeswax. The more color deviation (ΔE) is expected with higher reflux times. As the result of artificial aging, preservability of two dewaxed papers except of DP_SE(C) sample was higher than that of untreated paper i.e. beeswax-treated paper.

발행기관:
한국펄프·종이공학회
DOI:
http://dx.doi.org/10.7584/ktappi.2013.45.5.064
분류:
임학

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속실렛 추출법에 의한 밀랍지의 탈랍처리 효과분석 | 펄프종이기술 2013 | AskLaw | 애스크로 AI